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https://hdl.handle.net/10316/112592
Título: | Synthesis and Structural and Magnetic Properties of Polycrystalline GaMo4Se8 | Autor: | Malta, José F. Henriques, Marta S. C. Paixão, José A. Gonçalves, António P. |
Palavras-chave: | skyrmions; Jahn–Teller distortion; lacunar spinel; GaMo4Se8 | Data: | 2023 | Editora: | MDPI | Projeto: | José F. Malta’s PhD grant was supported by FCT-Fundação para a Ciência e a Tecnologia through the ChemMat PhD programme. Access to the TAIL-UC facility supported by the QREN-Mais Centro programme ICT_2009_02_012_1890 is gratefully acknowledged. This work was partially supported by funds from FEDER (Programa Operacional Factores de Competitividade COMPETE) and from FCT under the projects UIDB/FIS/04564/2020, UIDP/FIS/ 04564/2020 and PTDC/FISMAC/ 32229/2017. | Título da revista, periódico, livro ou evento: | Magnetochemistry | Volume: | 9 | Número: | 7 | Resumo: | GaMo4Se8, is a lacunar spinel where skyrmions have been recently reported. This compound belongs to the GaM4X8 family, where M is a transition metal (V or Mo) and X is a chalcogenide (S or Se). In this work, we have obtained pure GaMo4Se8 in polycrystalline form through an innovative two-step synthetic route. Phase purity and chemical composition were confirmed through the Rietveld refinement of the powder XRD pattern, the sample characterisation having been complemented with SEM analysis. The magnetic phase diagram was investigated using DC (VSM) and AC magnetometry, which disclosed the presence of cycloidal, skyrmionic and ferromagnetic phases in polycrystalline GaMo4Se8. | URI: | https://hdl.handle.net/10316/112592 | ISSN: | 2312-7481 | DOI: | 10.3390/magnetochemistry9070182 | Direitos: | openAccess |
Aparece nas coleções: | FCTUC Física - Artigos em Revistas Internacionais I&D CFis - Artigos em Revistas Internacionais |
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Ficheiro | Descrição | Tamanho | Formato | |
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Synthesis-and-Structural-and-Magnetic-Properties-of-Polycrystalline-GaMosub4subSesub8subMagnetochemistry.pdf | 3.89 MB | Adobe PDF | Ver/Abrir |
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