Please use this identifier to cite or link to this item: http://hdl.handle.net/10316/4838
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dc.contributor.authorMarques, E. P.-
dc.contributor.authorGil, F.-
dc.contributor.authorProença, P.-
dc.contributor.authorMonsanto, P.-
dc.contributor.authorOliveira, M. F.-
dc.contributor.authorCastanheira, A.-
dc.contributor.authorVieira, D. N.-
dc.date.accessioned2008-09-01T14:15:20Z-
dc.date.available2008-09-01T14:15:20Z-
dc.date.issued2000en_US
dc.identifier.citationForensic Science International. 110:2 (2000) 145-152en_US
dc.identifier.urihttp://hdl.handle.net/10316/4838-
dc.description.abstractThis paper describes an analytical method for strychnine determination in biological samples by gas chromatography/mass spectrometry and their application in the investigation of two cases involving strychnine ingestion: A fatal case and a clinical one. The strychnine is isolated from biological samples using a liquid-liquid extraction procedure. The clean-up procedure is performed using an acid solution. Papaverine is used as internal standard in the quantification of strychnine. In the analysed specimens, the limits of quantification were 0.1 [mu]g/ml or 0.1 [mu]g/g. The recovery rate ranged from 75.0% to 98.7% and the coefficients of variation ranged from 4.8% to 10.5%.en_US
dc.description.urihttp://www.sciencedirect.com/science/article/B6T6W-408KCFB-8/1/f8bbeefad9e20909aef50467f67a2e84en_US
dc.format.mimetypeaplication/PDFen
dc.language.isoengeng
dc.rightsopenAccesseng
dc.subjectStrychnineen_US
dc.subjectRodenticideen_US
dc.subjectAlkaloiden_US
dc.titleAnalytical method for the determination of strychnine in tissues by gas chromatography/mass spectrometry: two case reportsen_US
dc.typearticleen_US
item.languageiso639-1en-
item.grantfulltextopen-
item.fulltextCom Texto completo-
Appears in Collections:FMUC Medicina - Artigos em Revistas Internacionais
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